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Engineering, Energy, Transport AIC

space SCIENTIFIC JOURNALS OF VINNITSA NATIONAL AGRARIAN UNIVERSITY

Issue №: 2 (129)

Published: 2025.08.29
DOI: 10.37128/2520-6168-2025-2


Description:
The journal solves the problems of creation and improvement of machinery and technologies for agriculture: 131 - Applied Mechanics, 132 - Materials Science, 133 - Industrial Engineering, 141 - Power Engineering, Electrical Engineering and Electromechanics, 208 - Agricultural Engineering.

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STUDY OF THE METROLOGICAL CHARACTERISTICS OF A FLOW-TYPE MILK ACIDITY ANALYZER FOR MILKING EQUIPMENT

DOI: 10.37128/2520-6168-2025-2-2
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Elchyn ALIIEV – Doctor of Technical Sciences, Senior Researcher, Professor of the Department of Technical Systems Engineering of Dnipro State Agrarian and Economic University (St. S. Efremova, 25, Dnipro, Ukraine, 49000, e-mail: aliev@meta.ua, https://orcid.org/0000-0003-4006-8803). 
Volodymyr GOVORUKHA – Doctor of Physical and Mathematical Sciences, Professor, Head of the Department of Higher Mathematics, Physics and General Engineering Disciplines of Dnipro State Agrarian and Economic University (St. S. Efremova, 25, Dnipro, Ukraine, 49000, e-mail: hovorukha.v.b@dsau.dp.ua, https://orcid.org/0000-0002-0936-9272). 
Oleksandr PIVOVAROV – Doctor of Technical Sciences, Professor, Professor of the Department of Food Technologies of Dnipro State Agrarian and Economic University (St. S. Efremova, 25, Dnipro, Ukraine, 49000, e-mail: pivovarov.o.a@dsau.dp.ua, https://orcid.org/0000-0003-0520-171X).
Valentyn YEFIMOV – Candidate of Veterinary Sciences, Associate professor, Associate professor of the Department of Physiology, Biochemistry of Animals and Laboratory Diagnostics of Dnipro State Agrarian and Economic University (St. S. Efremova, 25, Dnipro, Ukraine, 49000, e-mail: yefimov.v.h@dsau.dp.ua, https://orcid.org/0000-0002-4286-8567).

Annotation

The paper presents the results of a study on the metrological characteristics of a flow-type milk acidity analyzer designed for integration into milking equipment to enable continuous real-time monitoring of raw milk quality. The relevance of this research is driven by the needs of modern livestock farming for the implementation of digital solutions within the framework of the Smart Farming concept. Milk acidity is a key indicator reflecting the microbiological status, freshness, and suitability of milk for processing, and its timely control allows for the prompt detection of hygienic violations during milking or early signs of animal diseases.
The proposed design of the flow analyzer is based on the ionometric method for measuring pH using a glass pH-selective electrode, a reference electrode, and a DS18B20 digital temperature sensor. The measuring unit is built on an ATMega16 microcontroller, integrated with a TL082 operational amplifier, which ensures high-precision measurement of the electrode system potentials. Signal processing and measurement control are implemented via PC software, which also provides electrode calibration, acidity calculation in pH and °T units, and digital and graphical visualization of results.
To determine the metrological characteristics of the analyzer, comparative measurements were carried out using a laboratory-grade pH meter S20 (Mettler Toledo) in buffer solutions with known pH values. It was established that the electrode response is linear with a slope of 59.62 mV/pH (theoretical value – 59.16 mV/pH), the measurement range is 1.68–9.18 pH, the signal dispersion is 3.00 mV², resolution – 0.01 pH, and the signal stabilization time – up to 25 seconds. The average deviation of the results does not exceed ±0.03 pH, which confirms compliance with the requirements for operational acidity monitoring in flow conditions.
The developed analyzer is competitive in terms of key metrological parameters and has strong potential for industrial application. Further research will focus on the implementation of automatic interpretation algorithms based on processing standards, as well as adaptation of the device to farms of various scales.

Keywords: milk, milk acidity, milking equipment, technical condition, pH meter, ionometric method, flow analyzer, metrological characteristics, quality control, automation, measurement.

List of references

1.    Kunes, R., Bartos, P., Iwasaka, G.K., Lang, A., Hankovec, T., Smutny, L., Cerny, P., Poborska, A., Smetana, P., Kriz, P., & Kernerova, N. (2021). In-Line Technologies for the Analysis of Important Milk Parameters during the Milking Process: A Review. Agriculture, 11(3), 239. DOI: 10.3390/agriculture11030239. [in English].
2.    Giannuzzi, D., Mota, L.F.M., Pegolo, S., Gallo, L., Schiavon, S., Tagliapietra, F., Katz, G., Fainboym, D., Minuti, A., Trevisi, E., & Cecchinato, A. (2022). In-line near-infrared analysis of milk coupled with machine learning methods for the daily prediction of blood metabolic profile in dairy cattle. Scientific Reports, 12, 8058. DOI: 10.1038/s41598-022-11799-0. [in English].
3.    Paliy, A., Aliiev, E., Paliy, A., Nechyporenko, O., Baidevliatova, Y., Baydevliatov, Y., Lazorenko, A., Ukhovskyi, V., Korniienko, L., & Sharandak, P. (2021). Determining the efficiency of cleaning a milk line made from different materials from contaminants. Eastern-European Journal of Enterprise Technologies, 4 (1 (112)), 76–85. DOI: 10.15587/1729-4061.2021.237070. [in English].
4.    Shevchenko, I., & Aliev, E. (2013). Automated control systems for technical processes in dairy farming. Annals of Warsaw University of Sciences, SGGW. Agriculture (Agricultural and Forest Engineering), 61, 41–49. [in English].
5.    Aliiev, E., Paliy, A., Dudin, V., Kis, V., Paliy, A., Ostapenko, V., Levchenko, I., Prihodko, M., Korg, O., & Kladnytska, L. (2022). Establishing an interconnection between the technical and technological parameters of milking equipment based on the movement of a milk-air mixture in a milking machine. Eastern-European Journal of Enterprise Technologies, 2 (1(116), 35–46. DOI: 10.15587/1729-4061.2022.253978. [in English].
6.    Liu, S., Contreras, F., Alemán, R. S., Fuentes, J. M., Arango, O., & Castillo, M. (2024). Validation of an Optical Technology for the Determination of pH in Milk during Yogurt Manufacture. Foods, 13(17), 2766. DOI: 10.3390/foods13172766. [in English].
7.    Aydogdu, T., O'Mahony, J. A., Huppertz, T., Magan, J. B., & McCarthy, N. A. (2023). Measuring pH of skim milk and milk permeate at ultra-high temperatures at laboratory and pilot scale. International Dairy Journal, 139, 105565. DOI: 10.1016/j.idairyj.2022.105565. [in English].
8.    Fernández González, A., Badía Laíño, R., Costa-Fernández, J. M., & Soldado, A. (2024). Progress and Challenge of Sensors for Dairy Food Safety Monitoring. Sensors, 24(5), 1383. DOI: 10.3390/s24051383. [in English].
9.    Aydogdu, T., O’Mahony, J.A., & McCarthy, N.A. (2023). pH, the Fundamentals for Milk and Dairy Processing: A Review. Dairy, 4(3), 395–409. DOI: 10.3390/dairy4030026. [in English].
10.    Voskoboynikova, O., Sukhanov, A., & Duerkop, A. (2021). Optical pH Sensing in Milk: A Small Puzzle of Indicator Concentrations and the Best Detection Method. Chemosensors, 9(7), 177. DOI: 10.3390/chemosensors9070177. [in English].
11.    Nanka, O., Shigimaga, V., Paliy, A., Sementsov, V., & Paliy, A. (2018). Development of the system to control milk acidity in the milk pipeline of a milking robot. Eastern-European Journal of Enterprise Technologies, 3 (9 (93)), 27–33. DOI: 10.15587/1729-4061.2018.133159. [in English].
12.    Chen, X., Yao, C., & Li, Z. (2023). Microarray-based chemical sensors and biosensors: Fundamentals and food safety applications, TrAC. Trends Anal. Chem, 158, 116785. DOI: 10.1016/j.trac.2022.116785. [in English].
13.    Tiwari, R., & Mahalpure, G.S. (2025). A Detailed Review of pH and its Applications. Journal of Pharmaceutical and Biopharmaceutical Research, 6(2), 492–505. DOI:10.25082/JPBR.2024.02.001. [in English].
14.    Megahed A.A., Hiew M., Grünberg W., Trefz F.M., & Constable P.D. (2019). Evaluation of the analytical performance of a portable ion-selective electrode meter for measuring whole-blood, plasma, milk, abomasal-fluid, and urine sodium concentrations in cattle. Journal of Dairy Science, 102(8), 7435–7444. DOI: 10.3168/jds.2018-16198. [in English].
15.    Ruiz-Gonzalez, A. (2024). Ion-Selective Electrodes in the Food Industry: Development Trends in the Potentiometric Determination of Ionic Pollutants. Electrochem, 5(2), 178–212. DOI: 10.3390/electrochem5020012. [in English].

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About journal

Topics of the journal:

131 - Applied Mechanics

132 - Materials Science

133 - Industry engineering

141 - Power engineering, electrical engineering and electromechanics

208 - Agricultural engineering

The magazine "Engineering, Energy, Transport AIC" is included in the list of scientific professional editions of Ukraine on technical sciences

(Category "Б", Order of the Ministry of Education and Science of Ukraine dated 02.07.2020 №886)

Old version of site: http://tetapk.vsau.edu.ua, http://techjournal.vsau.org

According to the decision of National Council of Television and Radio Broadcasting of Ukraine from 25.04.2024 No. 1337 the scientific journal «Engineering, Energy, Transport AIC» has the ID of the Media R30-05173.

The journal "Engineering, Energy, Transport AIC" is indexed according to the following databases and catalogs:

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Key information:
ISSN (print): 2520-6168
DOI: 10.37128/2520-6168

Certificate of state registration of mass media: No. 21906-11806 P dated 03/12/2016.

Founder of the journal: Vinnytsia National Agrarian University

Editor-in-chief: Olexii TOKARCHUK - Candidate of Technical Sciences, Associate Professor, VNAU (Vinnytsia)

Deputy Editor-in-Chief: Vitalii YAROPUD - Candidate of Technical Sciences, Associate Professor, VNAU (Vinnytsia)

Executive Secretary: Yuriy POLIEVODA - Candidate of Technical Sciences, Associate Professor, VNAU (Vinnytsia)

Members of the Editorial Board:

Oleg TSURKAN – Doctor of Technical Sciences, Full Professor, Vinnytsia National Agrarian University (Ukraine)

Volodymyr BULGAKOV – Doctor of Technical Sciences, Full Professor, Acad. NAAS, National University of Life and Environmental Sciences of Ukraine (Ukraine)

Rostislav ISKOVICH-LOTOTSKY  – Doctor of Technical Sciences, Full Professor, Vinnytsia National Technical University (Ukraine)

Yuliia SALENKO – Doctor of Technical Sciences, Full Professor, Kremenchuk Mykhailo Ostrohradskyi National University (Ukraine)

Igor KUPCHUK – Candidate of Technical Sciences, Associate Professor, Vinnytsia National Agrarian University (Ukraine)    

Serhii SHARHORODSKYI – Candidate of Technical Sciences, Associate Professor, Vinnytsia National Agrarian University (Ukraine)

Valerii HRANIAK – Candidate of Technical Sciences, Associate Professor, Vinnytsia National Agrarian University (Ukraine)

Anatoly SPIRIN – Candidate of Technical Sciences, Associate Professor, Vinnytsia National Agrarian University (Ukraine)

Olena SOLONA  – Candidate of Technical Sciences, Associate Professor, Vinnytsia National Agrarian University (Ukraine)

Igor TVERDOKHLIB – Candidate of Technical Sciences, Associate Professor, Vinnytsia National Agrarian University (Ukraine)

Yaroslav IVANCHUK – Doctor of Technical Sciences, Full Professor, Vinnytsia National Technical University (Ukraine)

Foreign members of the editorial board

Jordan Todorov MAXIMOV – Doctor of Technical Sciences, Full Professor, Technical University of Gabrovo (Bulgaria)   

Audrius ŽUNDA – Ph.D., Associate Professor, Vytautas Magnus University (Kaunas, Lithuania)

 

Type of publication: journal

Kind of publication: scientific

Publication status: domestic

Year of foundation: 1997

Periodicity: 4 times per year

Volume: 18-20 conv. print. sheet (А4)

ISSN: 2520-6168 (print version), (online version)

Language of publication: (mixed languages) Ukrainian, English

The sphere of distribution and category of readers: national, foreign, faculty, scientists, entrepreneurs.

The periodical edition is included to the List of scientific professional publications of Ukraine on technical sciences, approved by order of the Ministry of Education and Science of Ukraine in 05.16.2016, No. 515.

The journal "Engineering, Energy, Transport AIC" is included in the "Catalog of Ukrainian Publications".

Subscription to the journal can be issued in each post office. The subscription index is 99720.

History of journal:

It was founded in 1997 under the title "Bulletin of the Vinnitsa State Agricultural Institute." According to the Decree of the Presidium of the Higher Attestation Commission of Ukraine of September 11, 1997, this publication received the status of a professional in which it is allowed to publish the main results of dissertation researches.

In 2001-2014 the journal published under the title “Collection of scientific works of Vinnytsia National Agrarian University. Series: Technical Sciences "(Certificate of State Registration of Mass Media KV No. 16644-5116 PR of 04/30/2010).

Since 2015 journal has title "Engineering, Energy, Transport AIC" (Certificate of State Registration of Mass Media No. 21906-11806 P dated 03/12/2016).